Skip to main navigation menu Skip to main content Skip to site footer

Volatile compounds and their relation with differenciated coffee quality by wet processing Compuestos volátiles y su relación con la calidad del café diferenciado en el procesamiento vía húmeda

How to Cite
Osorio, V., Ortiz, A., Imbachi, L. C., & Fernández-Alduenda, M. R. (2026). Volatile compounds and their relation with differenciated coffee quality by wet processing. Cenicafe Journal, 77(1), e77103. https://doi.org/10.38141/10778/77103

Dimensions
PlumX

Keywords
Fruity

ripeness

quality

fermentation

time

temperature

coffee

Frutal

madurez

calidad

fermentación

fermento

tiempo

temperatura

Café

frutado

maturação

qualidade

fermentação

sabor fermentado

tempo

temperatura

café

Sectión
Articles

Summary

Coffee contains more than one thousand volatile compounds, of which approximately  thirty play a key role in the perception of beverage sensory attributes and are considered  major determinants of cup quality. The precursors of these compounds are formed during  coffee cultivation and postharvest processing and are subsequently transformed during  roasting through multiple chemical reactions. Among the most relevant classes of volatile  compounds are furans, pyrazines, organic acids, alcohols, and aldehydes. The composition  and relative abundance of these compounds enable discrimination between high-quality  coffees and those presenting sensory defects. This study evaluated 48 volatile compounds  in coffee beans obtained from fruits harvested at three ripening stages and subjected to  fruit reserve and prolonged mucilage fermentation. Fruit reserve significantly modified the  concentrations of compounds such as ethyl acetate, acetic acid, and ethanol, contributing  to the development of fruity and red-fruit sensory notes, particularly after 48 h of reserve.  In contrast, prolonged mucilage fermentation of fruits at advanced ripening stages and  under higher fermentation temperatures reduced the scores of five sensory attributes  and promoted fermenting flavor defect which is commonly associated with increased  concentrations of volatile compounds such as hexanal and 3-methylbutanoic acid.

Valentina Osorio, National Coffee Research Center

 Investigador Científico II. Calidad, Centro Nacional de Investigaciones de Café


Aristófeles Ortiz, National Coffee Research Center

Investigador Científico I. Fisiología, Cenicafé


Luis Carlos Imbachi, National Coffee Research Center

Asistente de Investigación. Biometría, Cenicafé


Mario Roberto Fernández-Alduenda, Specialty Coffee Association

Director Técnico. Specialty Coffee Association


References (See)

  1. Aswathi, K. N., Shirke, A., Praveen, A., & Murthy, P. S. (2024). Functioning of Saccharomyces cerevisiae in honey coffee (Coffea canephora) and their effect on metabolites, volatiles and flavor profiles. Food Research International, 180, 114092. https://doi.org/10.1016/j.foodres.2024.114092
  2. Avallone, S., Guiraud, J.-P., Guyot, B., Olguin, E., & Brillouet, J.-M. (2001). Fate of Mucilage Cell Wall Polysaccharides during Coffee Fermentation. Journal of Agricultural and Food Chemistry, 49(11), 5556-5559. https://doi.org/10.1021/jf010510s
  3. Batista Da Mota, M. C., Batista, N. N., Rabelo, M. H. S., Ribeiro, D. E., Borém, F. M., & Schwan, R. F. (2020). Influence of fermentation conditions on the sensorial quality of coffee inoculated with yeast. Food Research International, 136, 109482. https://doi.org/10.1016/j.foodres.2020.109482
  4. Burdock, G. A. (2016). Fenaroli’s Handbook of Flavor Ingredients (6a ed.). CRC Press. https://doi.org/10.1201/9781439847503
  5. Caporaso, N., Whitworth, M. B., Cui, C., & Fisk, I. D. (2018). Variability of single bean coffee volatile compounds of Arabica and robusta roasted coffees analysed by SPME-GC-MS. Food Research International, 108, 628-640. https://doi.org/10.1016/j.foodres.2018.03.077
  6. Cascos, G., Lozano, J., Montero-Fernández, I., Marcía-Fuentes, J. A., Aleman, R. S., Ruiz-Canales, A., & Martín-Vertedor, D. (2023). Electronic Nose and Gas Chromatograph Devices for the Evaluation of the Sensory Quality of Green Coffee Beans. Foods, 13(1), 87. https://doi.org/10.3390/foods13010087
  7. Caixeta, I. F., Guimarães, R. M., & Malta, M. R. (2013). Qualidade da semente de café pelo retardamento do processamento pós-colheita. Coffee Science, 8(3), 249-255. https://coffeescience.ufla.br/index.php/Coffeescience/article/view/425
  8. Chambers, E., & Koppel, K. (2013). Associations of Volatile Compounds with Sensory Aroma and Flavor: The Complex Nature of Flavor. Molecules, 18(5), 4887-4905. https://doi.org/10.3390/molecules18054887
  9. Clarke, R. J., & Vitzthum, O. G. (Eds.). (2001). Coffee: Recent developments. Wiley-Blackwell. http://doi.org/10.1002/9780470690499
  10. De Bruyn, F., Zhang, S. J., Pothakos, V., Torres, J., Lambot, C., Moroni, A. V., Callanan, M., Sybesma, W., Weckx, S., & De Vuyst, L. (2017). Exploring the Impacts of Postharvest Processing on the Microbiota and Metabolite Profiles during Green Coffee Bean Production. Applied and Environmental Microbiology, 83(1), e02398-16. https://doi.org/10.1128/AEM.02398-16
  11. Dippong, T., Dan, M., Kovacs, M. H., Kovacs, E. D., Levei, E. A., & Cadar, O. (2022). Analysis of Volatile Compounds, Composition, and Thermal Behavior of Coffee Beans According to Variety and Roasting Intensity. Foods, 11(19), 3146. https://doi.org/10.3390/foods11193146
  12. Do Carmo, K. B., Carmo, J. C. B. D., Krause, M. R., & Peterle, G. (2020). Sensory and physiological quality of arabic coffee under different fermentation times. Bioscience Journal, 36(2), 429-438. https://doi.org/10.14393/BJ-v36n2a2020-43255
  13. Evangelista, S. R., Silva, C. F., Miguel, M. G. P. D. C., Cordeiro, C. D. S., Pinheiro, A. C. M., Duarte, W. F., & Schwan, R. F. (2014). Improvement of coffee beverage quality by using selected yeasts strains during the fermentation in dry process. Food Research International, 61, 183-195. https://doi.org/10.1016/j.foodres.2013.11.033
  14. Galarza, G., & Figueroa, J. G. (2022). Volatile Compound Characterization of Coffee (Coffea arabica) Processed at Different Fermentation Times Using SPME-GC-MS. Molecules, 27(6), 2004. https://doi.org/10.3390/molecules27062004
  15. Kulapichitr, F., Borompichaichartkul, C., Pratontep, S., Lopetcharat, K., Boonbumrung, S., & Suppavorasatit, I. (2017). Differences in volatile compounds and antioxidant activity of ripe and unripe green coffee beans ( Coffea arabica L. ‘Catimor’). Acta Horticulturae, (1179), 261-268. https://doi.org/10.17660/ActaHortic.2017.1179.41
  16. Marie, L., Breitler, J.-C., Bamogo, P. K. A., Bordeaux, M., Lacombe, S., Rios, M., Lebrun, M., Boulanger, R., Lefort, E., Nakamura, S., Motoyoshi, Y., Mieulet, D., Campa, C., Legendre, L., & Bertrand, B. (2024). Combined sensory, volatilome and transcriptome analyses identify a limonene terpene synthase as a major contributor to the characteristic aroma of a Coffea arabica L. specialty coffee. BMC Plant Biology, 24(1), 238. https://doi.org/10.1186/s12870-024-04890-3
  17. Marwani, E., Syamsudin, T. S., Awaliyah, S., Maulani, R. R., Hidayat, A., Husyari, U. D., & Widiyanto, S. (2024). Volatile Metabolite Profiles of Robusta Green Bean Coffee From Different Geographical Origins in West Java and Their Correlation With Temperature, Rainfall, and Altitudes Using SPME GC-MS-Based Metabolomics. International Journal of Food Science, 2024(1), 6908059. https://doi.org/10.1155/2024/6908059
  18. Osorio, V., Álvarez-Barreto, C. I., Matallana, L. G., Acuña, J. R., Echeverri, L. F., & Imbachí, L. C. (2022). Effect of Prolonged Fermentations of Coffee Mucilage with Different Stages of Maturity on the Quality and Chemical Composition of the Bean. Fermentation, 8(10), 519. https://doi.org/10.3390/fermentation8100519
  19. Osorio, V., Matallana, L. G., Fernandez, M. R., Alvarez, C. I., Gallego, C. P., & Montoya, E. C. (2023). Chemical Composition and Sensory Quality of Coffee Fruits at Different Stages of Maturity. Agronomy, 13(2), 341. https://doi.org/10.3390/agronomy13020341
  20. Peñuela-Martínez, A. E., Pabón, J., & Sanz-Uribe, J. R. (2013). Método fermaestro: Para determinar la finalización de la fermentación del mucílago de café. Avances Técnicos Cenicafé, 431, 1-8. https://doi.org/10.38141/10779/0431
  21. Peñuela-Martínez, A. E., Zapata-Zapata, A. D., & Durango-Restrepo, D. L. (2018). Performance of different fermentation methods and the effect on quality coffee (Coffea arabica L.). Coffee Science, 13(4), 465. https://doi.org/10.25186/cs.v13i4.1486
  22. Sarghini, F., Fasano, E., De Vivo, A., & Tricarico, M. C. (2019). Influence of Roasting Process in Six Coffee Arabica Cultivars: Analysis of Volatile Components Profiles. Chemical Engineering Transactions, 75, 295-300. https://doi.org/10.3303/CET1975050
  23. Specialty Coffee Association. (2004). Cupping Protocols. Protocols & Best Practices. https://sca.coffee/research/protocols-best-practices
  24. Tsegay, G., Redi-Abshiro, M., S. Chandravanshi, B., Ele, E., M. Mohammed, A., & Mamo, H. (2019). Volatile profile of green coffee beans from Coffea arabica L. plants grown at different altitudes in Ethiopia. Bulletin of the Chemical Society of Ethiopia, 33(3), 401-413. https://doi.org/10.4314/bcse.v33i3.2
  25. Várady, M., Tauchen, J., Franková, A., Kloucek, P., & Popelka, P. (2022). Effect of method of processing specialty coffee beans (natural, washed, honey, fermentation, maceration) on bioactive and volatile compounds. LWT, 172, 114245. https://doi.org/10.1016/j.lwt.2022.114245
  26. Velmourougane, K., Bhat, R., Gopinandhan, T. N., & Panneerselvam, P. (2011). Impact of delay in processing on mold development, ochratoxin-A and cup quality in arabica and robusta coffee. World Journal of Microbiology and Biotechnology, 27(8), 1809-1816. https://doi.org/10.1007/s11274-010-0639-5
  27. Vezzulli, F., Lambri, M., & Bertuzzi, T. (2023). Volatile Compounds in Green and Roasted Arabica Specialty Coffee: Discrimination of Origins, Post-Harvesting Processes, and Roasting Level. Foods, 12(3), 489. https://doi.org/10.3390/foods12030489
  28. Wie, L., Tay, G. Y., Cheong, M. W., Curran, P., Yu, B., & Liu, S. Q. (2017). Modulation of the volatile and non-volatile profiles of coffee fermented with Yarrowia lipolytica: II. Roasted coffee. LWT, 80, 32-42. https://doi.org/10.1016/j.lwt.2017.01.070
  29. Wu, H., Gonzalez Viejo, C., Fuentes, S., Dunshea, F. R., & Suleria, H. A. R. (2024). Evaluation of spontaneous fermentation impact on the physicochemical properties and sensory profile of green and roasted arabica coffee by digital technologies. Food Research International, 176, 113800. https://doi.org/10.1016/j.foodres.2023.113800
  30. Yang, N., Liu, C., Liu, X., Degn, T. K., Munchow, M., & Fisk, I. (2016). Determination of volatile marker compounds of common coffee roast defects. Food Chemistry, 211, 206-214. https://doi.org/10.1016/j.foodchem.2016.04.124
  31. Yusianto, & Nugroho, D. (2014). Physical and Flavor Profiles of Arabica Coffee as Affected by Cherry Storage Before Pulping. Pelita Perkebunan, 30(2), 137-158. https://doi.org/10.22302/iccri.jur.pelitaperkebunan.v30i2.7
  32. Zhang, K., Cheng, J., Hong, Q., Dong, W., Chen, X., Wu, G., & Zhang, Z. (2022). Identification of changes in the volatile compounds of robusta coffee beans during drying based on HS-SPME/GC-MS and E-nose analyses with the aid of chemometrics. LWT, 161, 113317. https://doi.org/10.1016/j.lwt.2022.113317
  33. Zhang, Y., Li, X., Lo, C.-K., & Guo, S.-T. (2010). Characterization of the Volatile Substances and Aroma Components from Traditional Soypaste. Molecules, 15(5), 3421-3427. https://doi.org/10.3390/molecules15053421

Most read articles by the same author(s)

1 2 3 > >>